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Wuhan Circle Star Chem-medical Technology co.,Ltd.

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Wuhan Circle Star Chem-medical Technology co.,Ltd.

Business Type:Lab/Research institutions

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Main Products:
electronic chemicals, pharmaceutical intermediates, pesticide intermediates, ultraviolet absorbent, food additives
Year Established:
2023
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Wuhan Circle Star Chem-medical Technology co.,Ltd.

Country: China (Mainland)

Business Type:Lab/Research institutions

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2-Ethylhexyl salicylate

CAS NO.118-60-5

  • msdsMSDS/COA Download

  • Min.Order: 1 Kilogram
  • Payment Terms: L/C,D/A,D/P,T/T,MoneyGram,Other
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Product Details

Keywords

  • SALICYLIC ACID OCTYL ESTER
  • 2-ETHYLHEXYL SALICYLATE 99+%
  • SALICYLIC ACID 2-ETHYLHEXYL ESTER

Quick Details

  • ProName: 2-Ethylhexyl salicylate
  • CasNo: 118-60-5
  • Molecular Formula: C15H22O3
  • Appearance: liquid
  • Application: Pharma;Industry;Agricultural;chemical ...
  • DeliveryTime: 1-2 weeks after confirm order
  • PackAge: 25kg,50kg,180kg,200kg,250kg,1000kg,cus...
  • Port: Any port in China
  • ProductionCapacity: 15 Metric Ton/Month
  • Purity: 99%+
  • Storage: Keep it in dry,shady and cool place
  • Transportation: Transit could be DHL,UPS,TNT,EMS,Fedex...
  • LimitNum: 1 Kilogram
  • Moisture Content: COA mentioned
  • Impurity: COA mentioned

Superiority

1,we produce and sell good chemicals around the world.
2,our success rate is about 95%. this means, if customer order is accepted, the probability that the customer will obtain the ordered substances, is 95%.
3,our staff consists of highly qualified individuals with bsc, msc and ph.d degrees in chemistry, as well as excellent carbohydrates,nucleosides, small molecules and rare chemicals.
4,imaginechem's chemists are skilled at performing complex, multi-step syntheses and solving difficult chemistry-related problems. because of our better, concentracted size and low overheads, we are able to offer prompt quotations, very competitive prices, high quality products and fast delivery.
5,all chemicals are typically >97% for building blocks, the structure and purity is confirmed by nmr and lc-ms. intermediates and final products are analyzed by gc, hplc, ir, nmr, ms, elemental analysis, atom-absorpting analysis and crystallographical methods.
165,Customers-oriented strategy, exclusive supply chain management, professional R&D team, experienced production workers, energetic sales team enable us to offer best service andgood-value products to all of our customers and gradually reach our final goals: becoming global leading supplier for portable products and solutions.

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Isooctyl salicylate (also known as 2-ethylamyl salicylate) is an important chemical product, the appearance of colorless to light yellow transparent liquid, slightly aromatic smell, UVB(Chinese: Outdoor ultraviolet (UV) has absorption, widely used in perfume, soap, sunscreen cosmetics, pharmaceutical industry, can also be used as organic solvents and organic synthesis intermediates, at present China mainly relies on imports. In the first step of preparation, isoctyl alcohol solution with purity of 70%-99.9% was added to methyl salicylate solution with purity of 70%-99.9%, and the molar ratio of methyl salicylate in methyl salicylate solution and isoctyl alcohol in isoctyl alcohol solution was 1:1 to 1:3, stirring for 1 to 3 hours to form a evenly mixed raw material solution. As a preference, in the first stage, the molar ratio of methyl salicylate in methyl salicylate solution to isooctanol in isooctanol solution is 1:2. The second step is to add a solid inorganic alkali catalyst to the raw material solution prepared in the first step, and the quality of the inorganic alkali catalyst is 0.2% - 1.0% of the mass of the raw material solution to form a reaction solution. In the second step, the inorganic base catalyst is sodium hydroxide (NaOH) or potassium hydroxide (KOH). As a preferred option, the mass of the inorganic base catalyst is 0.5% of the total mass of the raw material solution. In the third step, the reaction solution Chemicalbook prepared in the second step was heated to 100-200 °C, and stirred for 4 to 10 hours after reaction, cooling the reaction solution to 2(T80°C), washing the reaction solution with hot water at a temperature of 50-100°C, separating and extracting the organic phase. In the second step, the methanol is recovered after a reaction of 4 to 10 hours. The reaction solution is heated to 100-200 °C to produce methanol gas. The methanol produced in the transesterification process of inorganic alkali catalyst and raw material solution was recovered by a recovery device. As a preferred option, the reaction solution is heated to 150°C. The stirring reaction time is 5 hours. Wash the reaction solution in hot water twice or three times. Step 4: First, add anhydrous Na2SO4 to the organic phase extracted in the third step, dry the organic phase with anhydrous Na2SO4, and remove the Na2SO4 in the organic phase after standing for 8-12 hours; Then, the organic phase with Na2SO4 removed was added to the flask, the oil pump was distilled under pressure, and the fraction of 174-178 °C/1.0kPa was collected as isooctanyl salicylate. In the fourth step, vacuum distillation of the oil pump is the prior art. 174-178 °C/1.0kPa indicates that the pressure gauge of the oil pump shows 1.0kPa, and the thermometer in the container containing the organic phase shows 174-178 °C